By Joseph Wang(auth.)
Chapter 1 primary recommendations (pages 1–27):
Chapter 2 research of Electrode Reactions (pages 28–59):
Chapter three Controlled?Potential thoughts (pages 60–99):
Chapter four sensible concerns (pages 100–139):
Chapter five Potentiometry (pages 140–170):
Chapter 6 Electrochemical Sensors (pages 171–202):
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Content material: bankruptcy 1 basic recommendations (pages 1–27): bankruptcy 2 research of Electrode Reactions (pages 28–59): bankruptcy three managed? capability innovations (pages 60–99): bankruptcy four sensible issues (pages 100–139): bankruptcy five Potentiometry (pages 140–170): bankruptcy 6 Electrochemical Sensors (pages 171–202):
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Additional resources for Analytical Electochemistry, Second Edition
Reversible electron transfer followed by a reversible chemical reaction, Er Cr mechanism: O neÀ R kt R 23 Z kÀ1 3. Reversible electron transfer followed by an irreversible chemical reaction, Er Ci mechanism: O neÀ R k R 23 Z 4. Reversible chemical reaction preceding a reversible electron transfer, Cr Er mechanism: k1 Z 23 O kÀ1 À O ne R 5. Reversible chemical reaction preceding an irreversible electron transfer, Cr Ei mechanism: k1 Z 23 O kÀ1 À O ne R 6. Reversible electron transfer followed by an irreversible regeneration of starting materials, catalytic mechanism: O neÀ R k R Z À3 O 7.
Further discussion of the electrical double layer can be found in several reviews (5,7±11). 1-4 ELECTROCAPILLARY EFFECT Electrocapillarity is the study of the interfacial tension as a function of the electrode potential. Such a study can provide useful insight into the structure and properties of 1-4 ELECTROCAPILLARY EFFECT 23 the electrical double layer. The in¯uence of the electrode±solution potential difference upon the surface tension (g) is particularly pronounced at nonrigid electrodes (such as the dropping mercury electrode discussed in Section 4-5).
The extra potential beyond the equilibration potential leading to a net current i). The overvoltage is always de®ned with respect to a speci®c reaction, for which the equilibrium potential is known. Equation (1-26) can be used for extracting information on i0 and a, which are important kinetic parameters. For suf®ciently large overvoltages (Z > 118 mV=n), one of the exponential terms in equation (1-26) will be negligible compared with the other. For example, at large negative overpotentials, ic ) ia and equation (1-26) becomes i i0 exp ÀanFZ=RT 1-27 ln i ln i0 À anFZ=RT 1-28 and hence we get This logarithmic current±potential dependence was derived by Tafel, and is known as the Tafel equation.
Analytical Electochemistry, Second Edition by Joseph Wang(auth.)